One of the features that made Scientific American magazine great was a column called “The Amateur Scientist.” Every month, readers were treated to experiments that could be done at home, or some scientific apparatus that could be built on the cheap. Luckily, [Ben Krasnow]’s fans remember the series and urged him to tackle a build from it: a DIY mass spectrometer. (Video, embedded below the break.)
[Ben] just released the video below showing early experiments with a copper tube contraption that was five months in the making; it turns out that analytical particle physics isn’t as easy as it sounds. The idea behind mas spectrometry is to ionize a sample, accelerate the ions as they pass through a magnetic field, and measure the deflection of the particles as a function of their mass-to-charge ratio. But as [Ben] discovered, the details of turning a simple principle into a working instrument are extremely non-trivial.
His rig uses filaments extracted from carefully crushed incandescent lamps to ionize samples of potassium iodide; applied to the filament and dried, the salt solution is ionized when the filament is heated. The stream of ions is accelerated by a high-voltage field and streamed through a narrow slit formed by two razor blades. A detector sits orthogonal to the emitter across a powerful magnetic field, with a high-gain trans-impedance amplifier connected. With old analog meters and big variacs, the whole thing has a great mad scientist vibe to it that reminds us a bit of his one-component interferometer setup.
[Ben]’s data from the potassium sample agreed with expected results, and the instrument is almost sensitive enough to discern the difference ..
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